Characteristics of High Nb Containing TiAl Alloyed Powders by Radio Frequency Plasma Processing

LU Xin;WANG Shu-chao;ZHU Lang-ping;HE Xin-bo;HAO Jun-jie;QU Xuan-hui

Journal of Aeronautical Materials ›› 2011, Vol. 31 ›› Issue (4) : 1-6.

PDF(1190 KB)
PDF(1190 KB)
Journal of Aeronautical Materials ›› 2011, Vol. 31 ›› Issue (4) : 1-6.

Characteristics of High Nb Containing TiAl Alloyed Powders by Radio Frequency Plasma Processing

Author information +
History +

Abstract

Ti-45Al-8.5Nb-0.2W-0.2B-0.02Y(at%) ingot was prepared using a vacuum induction furnace,and then machined with a crusher in argon atmosphere.Subsequently,microfine spherical high Nb containing TiAl alloyed powders were obtained by fluidized bed jet milling in inert gas and then by radio frequency argon plasma.The fabrication process and characteristics of the powders were investigated.The results show that the powders fabricated by this process is highly refined and spheroidized,and the particle size is accurately controlled in a small interval.The plasma-spheroidized powders are dominated by α2-Ti3Al with a minor amount of β-Ti2AlNb.The oxygen content becomes higher gradually with the decrease of the particle size.The exterior and interior microstructures of the alloyed powders strongly depend on the particle size.The powders with an average particle size of 90μm show dendritic microstructure,and network Al-rich phase segregation exists within the particles.With the particle size decreasing,the surface of the powders tends to be smooth,and the internal segregation is gradually weakened.In addition,the 90μm powders possess high composition homogeneity,and with the decrease of the particle size the composition homogeneity declines gradually.

Key words

high Nb containing T / spherical powder / radio frequency plas / powder characteristi

Cite this article

Download Citations
LU Xin, WANG Shu-chao, ZHU Lang-ping, HE Xin-bo, HAO Jun-jie, QU Xuan-hui. Characteristics of High Nb Containing TiAl Alloyed Powders by Radio Frequency Plasma Processing[J]. Journal of Aeronautical Materials, 2011, 31(4): 1-6

References

KIM Y W.Ordered intermetallic alloys,part 3:gamma titanium aluminides[J].JOM,1994,46(7):30-39.
WANG Y H,LIU J P,HE Y H,et al.Microstructure and mechanical properties of as-cast Ti-45Al-8.5Nb-(W,B,Y)alloy with industrial scale[J].Material Science and Engineering (A),2007,471 (1~2):82-87.
YOSHINARA M,MIURA K.Effect of Nb on oxidation behavior of TiAl[J].Intermetallics,1995,3 (5):357-363.
PAUL J D H,APPEL F,WANGER R.The compression behavior of niobium alloyed γ-titanium aluminides[J].Acta Materialia,1998,46(4):1075-1085.
CHEN G L,ZHANG W J,LIU Z C,et al.Microstructure and properties of high-Nb containing TiAl-based alloys[C]// KIM Y W,DIMIDUK D M,LORETTO M H.Gamma Titanium Aluminides.Warrendale PA USA:TMS,1999:371-380.
CHEN G L,LIN J P,SONG X P,et al.Development of high Nb containing high temperature TiAl alloys[C]// KIM Y W,CARNEIRO T.Proceedings of the International Symposium on Niobium for High Temperature Applications.Warrendale PA USA:TMS,2004:153-166.
LIU Z C,LIN J P,LI S J,et al.Effects of Nb and Al on the microstructures and mechanical properties of high Nb containing TiAl base alloys[J].lntermetallics,2002,10(7):653-659.
李书江.高铌TiAl微合金化及蠕变性能[D].北京:北 京科技大学.2001.
THOMAS M,RAVIART J L,POPOFF F.Cast and PM processing development in gamma aluminides[J].Intermetallics,2005,13 (9):944-951.
HSIUNG L M,NIEH T G.Microstructures and properties of powder metallurgy TiA1 alloy[J].Materials Science and Engineering (A),2004,364 (1 ~2):1-10.
BOUYER E,GITZHOFER F,BOULOS M I.Suspension plasma spraying for hydroxyapatite powder preparation by RF plasma[J].IEEE Transactions on Plasma Science,1997,25(5):1066-1072.
SUN X L,TOK A I Y,HUEBNER R,et al.Phase transformation of ultrafine rare earth oxide powders synthesized by radio frequency plasma spraying[J].Journal of the European Ceramic Society,2007,27(1):125-130.
STEPHENS R L,MCFEATERS J S,WU M K,et al.The synthesis of ultrafine engineering ceramic powders using an RF plasma torch[C]//Chemeca 90:The Eighteenth Australasian Chemical Engineering Conference:Processing Pacific Resources.Auckland N Z:Chemical Engineering Group,1990:470-476.
SEOJ H,KIM D U,NAM J S,et al.Radio frequency thermal plasma treatment for size reduction and spheroidization of glass powders used in ceramic electronic devices[J].Journal of the American Ceramic Society,2007,90(6):1717-1722.
WANG Y H,LIN J P,HE Y H,et al.Fabrication and SPS microstructures of Ti-45Al-8.5Nb-(W,B,Y) alloying powders[J].Intermetallics,2008,16(2):215-224.
PDF(1190 KB)

17

Accesses

0

Citation

Detail

Sections
Recommended

/